Homonuclear dipolar decoupling at magic-angle spinning frequencies up to 65 kHz in solid-state nuclear magnetic resonance

Michal Leskes; Stefan Steuernagel; Denis Schneider; P. K. Madhu; Shimon Vega

doi:10.1016/j.cplett.2008.10.029

Homonuclear dipolar decoupling at magic-angle spinning frequencies up to 65 kHz in solid-state nuclear magnetic resonance

Michal Leskes, Stefan Steuernagel, Denis Schneider, P. K. Madhu^*, Shimon Vega

^*Corresponding author for this work

Research output: Contribution to journal › Article › peer-review

62 Citations (Scopus)

Abstract

We report here high-resolution ¹H solid-state nuclear magnetic resonance spectra acquired by a combination of magic-angle spinning (MAS) and radiofrequency pulse methods up to MAS frequencies of 65 kHz. The details of the pulse methods and experimental conditions are outlined together with spectra from model compounds.

Original language	English
Pages (from-to)	95-99
Number of pages	5
Journal	Chemical Physics Letters
Volume	466
Issue number	1-3
DOIs	https://doi.org/10.1016/j.cplett.2008.10.029
Publication status	Published - 24 Nov 2008

Funding

Israel Science Foundation; PKM; Department of Science and Technology, India; SERC FAST Track SchemeWe acknowledge support from the Israel Science Foundation and PKM additionally acknowledges assistance from the Department of Science and Technology, India, under SERC FAST Track Scheme. The research is made possible in part by the historic generosity of the Harold Perlman family.

All Science Journal Classification (ASJC) codes

General Physics and Astronomy
Physical and Theoretical Chemistry

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10.1016/j.cplett.2008.10.029

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title = "Homonuclear dipolar decoupling at magic-angle spinning frequencies up to 65 kHz in solid-state nuclear magnetic resonance",

abstract = "We report here high-resolution 1H solid-state nuclear magnetic resonance spectra acquired by a combination of magic-angle spinning (MAS) and radiofrequency pulse methods up to MAS frequencies of 65 kHz. The details of the pulse methods and experimental conditions are outlined together with spectra from model compounds.",

author = "Michal Leskes and Stefan Steuernagel and Denis Schneider and Madhu, {P. K.} and Shimon Vega",

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AU - Leskes, Michal

AU - Steuernagel, Stefan

AU - Schneider, Denis

AU - Madhu, P. K.

AU - Vega, Shimon

PY - 2008/11/24

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AB - We report here high-resolution 1H solid-state nuclear magnetic resonance spectra acquired by a combination of magic-angle spinning (MAS) and radiofrequency pulse methods up to MAS frequencies of 65 kHz. The details of the pulse methods and experimental conditions are outlined together with spectra from model compounds.

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JO - Chemical Physics Letters

JF - Chemical Physics Letters

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Homonuclear dipolar decoupling at magic-angle spinning frequencies up to 65 kHz in solid-state nuclear magnetic resonance

Abstract

Funding

All Science Journal Classification (ASJC) codes

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